An official website of the United States government.

Official websites use .gov
A .gov website belongs to an official government organization in the United States.

Secure .gov websites use HTTPS
A lock ( ) or https:// means you've safely connected to the .gov website. Share sensitive information only on official, secure websites.

Research Publications (Food Safety)

This page tracks research articles published in national and international peer-reviewed journals. Recent articles are available ahead of print and searchable by Journal, Article Title, and Category. Research publications are tracked across six categories: Bacterial Pathogens, Chemical Contaminants, Natural Toxins, Parasites, Produce Safety, and Viruses. Articles produced by USDA Grant Funding Agencies (requires login) and FDA Grant Funding Agencies (requires login) are also tracked in Scopus.

Displaying 1 - 25 of 239

  1. Residue behaviors and dietary risk assessments of four field-applied pesticides in common food products derived from goji berries (Lycium barbarum L.)

    • Food Control
    • Lycium barbarum L., also known as goji berry, is popular in China and across the world as both a food and a medicine. The pervasive use of chemical pesticides has led to widespread contamination of raw goji berries, although the impacts of pesticide contamination on goji berry-derived products have not yet been thoroughly characterized.

      • Chemical contaminants
      • Pesticide residues
  2. The presence of antibiotic residues in raw milk samples obtained after the withdrawal period and other quality parameters in relation to selected factors

    • Food Control
    • The aim of this study was to compare the results of the presence of antibiotic (AB) residues in the milk of dairy cows treated with ABs – during the withdrawal period (WP) and after the WP obtained by various screening tests (Delvotest T, Twinsensor BT020, and Eclipse 50), to evaluate the presence of AB residues with regard to selected factors (indication for AB administration, AB group, and a number of antimicrobial substances) and to assess selected parameters of milk quality (fat, crude pr

      • Chemical contaminants
      • Antibiotic residues
  3. Processing factors of pesticide residues in cereal grain fractions

    • Food Control
    • This study examined the distribution of 37 pesticide residues in different cereal grains (rye, wheat, oat, and barley) and their fractions, including flour, bran, and feed bran. The grains used in the study were sprayed in the field before processing to provide a more accurate representation of the fate of pesticide residues in these fractions. Pesticides were extracted using the QuEChERS method and analyzed by GC-MS/MS and LC-MS/MS.

      • Chemical contaminants
      • Pesticide residues
  4. Formula model established through field application of glass slides and rapid analysis of pesticide residues in vegetables by ion mobility spectrometry

    • Food Control
    • The prevalence of pesticide usage has brought the matter of pesticide residues to the forefront, necessitating the development of effective detection methods as a crucial step towards addressing this issue. This study presents a novel approach for detecting pesticide residues in vegetables using glass slide-formula-ion mobility spectrometry (IMS). The approach enables swift analysis of 36 different pesticides across three vegetable species with glass slides.

      • Chemical contaminants
      • Pesticide residues
  5. Manufacturing practices as potential sources of cadmium and other relevant metals in processed meat products. Risk and nutritional assessment

    • Food Control
    • Processed meat products could constitute a relevant source of cadmium (Cd) and other toxic elements in the diet as they could contain organ meats (e.g. kidneys, liver) known to accumulate metals. Additionally, these products could be contaminated due to metal transfer from the machinery during processing and, in the case of canned meats, metal migration from the container could also occur.

      • Chemical contaminants
      • Heavy Metals
  6. Removal of six pesticide residues from vegetables by the coupled ultrasonic-ozonation process

    • Food Control
    • The presence of pesticide residues in vegetables is a worldwide issue regarding food safety. This study explores the efficacy of a novel advanced oxidation process (AOP), namely the coupled ultrasonic-ozonation (US/O3) process, for removing six commonly found pesticides from vegetables.

      • Chemical contaminants
      • Pesticide residues
  7. Food safety assessment of wines commercialised in the Canary Islands by monitoring of pesticide residues from 2017 to 2019

    • Food Control
    • Population growth, international market expansion, and climate change have caused changes in agricultural practices, including increased use of phytosanitary products to control pests and diseases in food production. The European Union aims to achieve sustainable and high-quality food, with the priority of reducing pesticide use.

      • Chemical contaminants
      • Pesticide residues
  8. Effect of different agricultural conditions, practices, and processing on levels of total arsenic and species in cereals and vegetables: A review

    • Food Control
    • Arsenic (As) is absorbed and accumulated during the growth of crops, resulting in elevated As concentrations in agricultural products, and threatening human health. Considering As toxicity is associated with chemical species, this review outlines the available literature on both total As and its species in agricultural products. The review reflects that inorganic As was the dominant species in cereal grains (42%–98%) and vegetables (84.2%–100%), the As species in mushrooms are diverse.

      • Chemical contaminants
      • Heavy Metals
  9. Simultaneous determination of various heavy metal and arsenic ions in seafood using functionalized fibrous silica (KCC-1) coated stir bar sorptive extraction prior to inductively coupled plasma mass spectrometry

    • Food Control
    • Heavy metal ions (HMIs) and arsenic ion with high bioavailability and toxicity in seafood pose a serious threat to human health by food chain.

      • Chemical contaminants
      • Heavy Metals
  10. Development and application of a rapid screening and quantification method for multi-class herbicide residues in fishery products using UPLC-Q-Tof-MS/MS: Evidence for prometryn residues in shellfish

    • Food Control
    • Quality and safety issues arising from herbicide residues in fishery products are a growing concern. In order to ensure the edible safety of fishery products, a comprehensive assessment of multi-class herbicide residues should be conducted. Hence a modified QuEChERS approach was explored and validated using UPLC-Q-Tof-MS/MS for rapid screening and quantification of 158 herbicide residues in fishery products.

      • Chemical contaminants
      • Pesticide residues
  11. Detection of antibiotic residues in chicken meat from different agro-climatic zones of Chhattisgarh, India by HPLC-PDA and human exposure assessment and risk characterization

    • Food Control
    • Antibiotic residues in chicken meat pose health risks to consumers and affect the economics of the poultry industry due to an export ban. The present cross-sectional study aimed to determine the occurrence of antibiotic residues in marketed chicken meat collected under different agro-climatic conditions in Chhattisgarh, India, and assess human health risks by Monte Carlo Simulation.

      • Chemical contaminants
      • Antibiotic residues
  12. Analysis of veterinary drug- and pesticide residues in pig muscle by LC-QTOF-MS

    • Food Control
    • A liquid chromatography-high resolution mass spectrometry (LC-HRMS) method for screening, quantification and identification of veterinary drugs (antibiotics, nonsteroidal anti-inflammatory drugs, anthelmintics, coccidiostatics and tranquilizers) and pesticide residues was validated in pig (porcine) muscle.

      • Chemical contaminants
      • Antibiotic residues
      • Pesticide residues
  13. Determination of 301 pesticide residues in tropical fruits imported to Turkey using LC–MS/MS and GC-MS

    • Food Control
    • This study was carried out to detect pesticide residues in tropical fruits. QuEChERS method was validated to determine 301 different pesticides in high water content commodities and high acid content commodities by liquid chromatography-tandem mass spectrometry (LC–MS/MS) and gas chromatography-mass spectrometry (GC-MS). Matrix effects were determined for all pesticides in banana, blueberry, lime, mango, and pineapple.

      • Chemical contaminants
      • Pesticide residues
  14. Quantitative determination of polychlorinated biphenyls in chicken based on QuEChERS extraction and GC-MS/MS detection

    • Food Control
    • Polychlorinated biphenyls (PCBs), a class of synthetic organic compounds consisting of chlorine atoms on two coupled biphenyl rings, have been declared class A carcinogens by the World Health Organization. Here, we report a new method for the determination of PCBs content in chicken.

      • Chemical contaminants
      • Dioxins
  15. Use of high-resolution mass spectrometry for veterinary drug multi-residue analysis

    • Food Control
    • National and international food and feed safety authorities are shifting from routine-to risk-based monitoring. Risk-based monitoring requires flexibility in the scope of analytes, matrices, and sampling. Also, risk-based monitoring implies a desire for retrospective analysis using different scope(s) to follow trends, identify new food safety threats, and monitor the effectiveness of policy interventions.

      • Chemical contaminants
      • Antibiotic residues
  16. Using low dose fungicide by combining with intermittent ozone treatment to reduce fungicide residue, microbial load and quality losses in orange fruit during long term storage

    • Food Control
    • In the present study, the effects of intermittent ozone (IO3) application combined with low dose fungicide and high-dose dissolved ozone in water on storage life and quality of orange cv. Washington Navel were investigated.

      • Chemical contaminants
      • Pesticide residues
  17. Detection and risk associated with organochlorine, organophosphorus, pyrethroid and carbamate pesticide residues in chicken muscle and organ meats in Jordan

    • Food Control
    • The aims of this study were to: i) analyze the prevalence and concentration of pesticides belonging to 4 major classes, namely organochlorines, organophosphates, carbamates and pyrethroids in chicken meat, liver and kidney; ii) evaluate the impact of boiling, frying and freezing on pesticide levels in chicken meat, and iii) estimate the dietary exposure to pesticide residues in chicken meat and conduct a risk assessment.

      • Chemical contaminants
      • Pesticide residues
  18. Thermochemical degradation investigation of pesticide residues in banana homogenate

    • Food Control
    • As a first-time study, the thermal storage stabilities of pesticides (bifenthrin, carbofuran, diazinon, methomyl, triflumuron, triadimenol, triazophos, and thiabendazole) in banana homogenate were investigated. Pesticides-spiked banana samples were stored at −20 °C (T1), 4 °C (T2), 25 °C (T3), and 40 °C (T4) and the residues were observed from day 0 to day 84.

      • Chemical contaminants
      • Pesticide residues
  19. The effect of food thermal processes on the residue concentration of systemic and non-systemic pesticides in apples

    • Food Control
    • The goal of the present study was to estimate the distribution and migration of eleven systemic and non-systemic pesticides between the skin and the pulp of apples. Additionally, the behaviour of acetamiprid, boscalid, bupirimate, cyprodinil, flonicamid, fluopyram, pirimicarb, pyrimethanil, thiacloprid, deltamethrin, and fludioxonil in two apple varieties during four thermal processes ranging between −40 °C and 150 °C was discussed.

      • Chemical contaminants
      • Pesticide residues
  20. Comparison of QuEChERS and Liquid–Liquid extraction methods for the simultaneous analysis of pesticide residues using LC-MS/MS

    • Food Control
    • In 2004, the Food Code of Korea adopted a multi-class multi-residue pesticide analysis method, which employed liquid–liquid extraction (LLE) and solid-phase extraction for sample purification. After several modifications, the LLE stage was replaced by the QuEChERS method in October 2021. Thus, in the current study a comparison was carried out between the new QuEChERS method and the conventional LLE method for the simultaneous analysis of multiple pesticide residues.

      • Chemical contaminants
      • Pesticide residues
  21. Determination of 43 pesticide residues in intact grape berries (Vitis Vinifera L.) by using an ultrasound-assisted acetonitrile extraction method followed by LC–MS/MS

    • Food Control
    • An ultrasound-assisted acetonitrile extraction method was applied for the determination of 43 pesticide residues in intact grape berries (Vitis Vinifera L.) by liquid chromatography-tandem mass spectrometry (LC–MS/MS). The results showed that ultrasound-assisted extraction from intact grape berries exhibited better efficiency than extraction from homogenized grape berries.

      • Chemical contaminants
      • Pesticide residues
  22. Application of saponins extract from food byproducts for the removal of pesticide residues in fruits and vegetables

    • Food Control
    • Vegetables and fruits may contain pesticides, leading to several health complications after long-term exposure. The food byproducts of soybean and camellia seed cake contain abundant saponins but are poorly utilized. This study aimed to investigate the capacity of soybean byproduct-extracted saponins (SBE) and camellia seed cake-extracted saponins (CSE) to remove pesticide residues in fruits and vegetables.

      • Chemical contaminants
      • Pesticide residues
  23. Investigation and analysis of pesticide residues in edible fungi produced in the mid-western region of China

    • Food Control
    • The present study sought to investigate the levels of multi-pesticide residues in highly consumed edible fungi in China's western regions. A total of 354 edible fungi samples were collected from the local markets, and the concentrations of 53 pesticides in these samples were determined through high performance liquid chromatography mass spectrometer (HPLC/MS/MS). Carbendazim, acephate, procymidone, prochloraz, aldicarb sulfone,etc.

      • Chemical contaminants
      • Pesticide residues
  24. Residues of veterinary drugs in fish and fish products: An analysis of RASFF data over the last 20 years

    • Food Control
    • An analysis of the notifications in the European Union (EU) Rapid Alert System for Food and Feed (RASFF) portal due to residues of veterinary drugs in fish and fish products over the period 2001–2021 was conducted examining the following data: number and type of notifications; year of notification; notification basis; notifying country; country of origin; action taken; distribution status; risk decision; fish product type; residue found.

      • Chemical contaminants
      • Antibiotic residues
  25. Prescreening veterinary drug residues, heavy metal concentration, and genetic authentication in retail catfish fillets in the Northeast United States

    • Food Control
    • Veterinary drug residues, heavy metals, and species authentication were performed on the demand of the regulatory agency in retail catfish fillets. A total of 362 domestic and imported catfish samples collected from various retail markets in the Northeast region of the United States were tested for the presence of chloramphenicol (CAP), malachite green/gentian violet (MG/GV), As, Cd, Pb, and Hg according to the USDA - FSIS protocols.

      • Chemical contaminants
      • Antibiotic residues